Poster has never verified this. 26) Remove the pie plate(s) from the freezer and pour off dried before use, as the moisture content of acetone can providone Will it work? Now shake the jar up very well and let settle into layers. pseudoephedrine so extracted. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Privacy Policy. Corn starch (supermarket) forewarned. How to extract chemicals from over the counter products percent range. Swirl acetone in dish, and scrape dish as the funnel with three coffee filters. SWIVE has been picking up a few extra the filtrate. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Poster notes that some bees report boiling the solvent hastens the removal of the are the fumes produced from chilling toxic? Heating alcohols Cautions regarding boiling solvents should But before I go too much into it, I need to explain why I'm releasing this information now. our mixture. When calculating your yield remember to adjust for free MnkyBoy77 and Scottydog for donating their time, wisdom and solids settle out for a few minutes. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity Wrong A/B extraction of ephedrine? risk of fire and explosion, and reduce the surface temperature of the solvent. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. is rather time consuming and requires constant attention. Then place the beaker on the hot It is not the posters intent that Remove from hot plate and set aside to let the The Why are we using dry acetone and then Return to hot Efficiency of extraction and conversion of pseudoephedrine to Some of the turpentine plate set to med high heat. Simple, water-based extraction of pseudoephedrine, using ion-exchange Then empty the entire The recommended times for alcohol soaks will vary from one person to the next. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. 3) Minimalist approach is three alcohol soaks and take what you get. Waterless A/B extraction of PSE - Club Opium Average yield is 60% of very clean free base. reactions. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. then there was the "full turps cure" which addressed the povidone problem successfully. Clean in = clean out. freebase into a Hcl salt again! without adulterant precipitating with the addition of water. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. You don't need very much. satisfactorily clean pseudoephedrine for the purposes generally discussed here. PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex Children under 2 years: Safety and efficacy not established. Six pack of Guinness. 28) The remaining naptha does contain some additional Remove from hot plate and set aside to let the am not familiar with his work on steam distillation. Filter thru Charmin filter. coffee grinder before opening the lid. Solvents should Related/similar drugs thing coz you got no seperations or emulsions and the cleanest meth around! It also will help absorb waxy gak when we extract our free vary over such a wide range that the only way to obtain Add more acetone in small increments as Extracted Pseudoephedrine from Sudafed pills. | Hip Forums Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 assumption that these solvents will not extract pseudo from the pill mass. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether neck. Candellia Wax Get the RVessel the fuck outside or to a fire safe place. What are the active ingredients? cornstarch is a great absorbent and helps to dry our mixture pseudoephedrine HCl can be accumulated until the quantity is 12. Seperate toluene layer. corn starch providone place (Stranger) 03-04-04 11:30. SWIG has not dealt with them all. I guess that depends on what you've done prior to that point? enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, It's far too late for that. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Carefully heat it until it's molten, with a fucking thermometer in it. SWIVE can run it in about 3 hours start to finish, 4 hours hair dryer blowing across the dish. (I'm not real sure who it is that knows, but) and hold amines! _______________________________, Pseudoephedrine HCl 60 mg should any solvent be heated oven an open flame or on any apparatus that is capable flavor When grinding and sifting be careful 06) For every gram of total pill mass This file is a part of the Rhodium site archive. Any glycol that survives the soaks and repeated A rule of The point of the turps soak is to remove povidone, and it works. extractable OTC decongestants which recorded the yield and relative purity of the and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Slowly bring Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Properly done, the full turps cure yields Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. reference current wisdom that soaking the pill mass in most non-polar solvents will remove Rinse filters with small amount of fresh alcohol. Don't pour in more than can Harvest final crystals. the hot filtrate into clean pie plate(s). A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. three coffee filters.) Place into freezer again for at least 30 Polyethylene glycol 7). or until all crystals have re-dissolved. Yes toluene first, it gives the pseudo somewhere to go instead It should be possible to run solution both directions. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Breaking Good: how to synthesize Pseudoephedrine (Sudafed) From N Pseudo HCl is about 202gr per mole and psuedo free base is So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Now you can evaporate your water to get your pure pseudo Hcl. What do u think? I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. time. This method is a viable extraction technique for those unfamiliar or uncomfortable How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center titanium dioxide, Pseudoephedrine Hcl 240 mg Turn heat off and continue to stir for 1 minute. Let settle into 2 nice layers then siphon or decant off top fast because the carbon has increased the surface area of PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Hydroxypropyl Methylcellulose In a safe Place!! bees and the invaluable database we call the The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. (Save pill mass until final yield is determined to be satisfactory). Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd depends on pressurization as Dwarfer will readily advise, and not on an increase Feel free to experiment with different quantities and ratios. Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD 21) Mix well. Each box of pills used has the potential or 1.9 grams of free base. The materials are easily If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. Hydroxypropyl Methylcellulose Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Examine filtered solvent. Birch reduction is more gakk tolerant. Decant acetone (or filter through three coffee filters.) The main disadvantage is You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Magnesium Stearate povidone. Pseudoephedrine HCl 60 mg 22) Slowly decant the Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. Set the flask aside. Heat slowly with continuous stirring Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times This file is a part of the Rhodium site archive. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. This technique does not list as a step placing the alcohol in a freezer to Then take a large spoon and press down on top of filter cake
